Faculty of Engineering
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Item Compositional Analysis and Characterisation of Non-edible Plant Biomass for Carboxymethyl Cellulose Production(IEEE, 2023-11-01) Hauwa A. Rasheed; Adekunle Akanni Adeleke; Petrus Nzerem; Ayuba Salihu; Temitayo Samson Ogedengbe; Peter Pelumi IkubanniThis study assesses the compositional analysis and characterization of eight non-edible plant biomass identified as a potential feedstock to produce carboxymethyl cellulose. The materials' contents were ascertained by gravimetric analysis, and they were further characterized using Fourier transforms Infrared spectroscopy. According to the research, cellulose was present in substantial amounts ranging from 33 % to 41 %, with sugarcane bagasse having the highest concentration. The percentage of hemicellulose ranged from 18 % to 28 %, with corn cob having the highest percentage. Also discovered was that lignin content varied between 9 % and 22 %, with mahogany having the highest amount amongst the samples. The FTIR spectroscopic analysis of all eight samples reveals a broad band at around 3300 cm-1, which is caused by the stretching vibration of the cellulose's O-H groups. The observed peaks at 1600 cm-1 and 1500 cm-1 correlated to the hemicellulose and lignin's respective C=O and C=C stretching vibrations. Additionally, a significant sharp peak that matched the stretching vibrations in the skeleton of the pyranose ring, C-O-C, was seen at roughly 1050 cm-1. Thus, the findings of this study indicate that all eight samples can yield a respectable amount of cellulose, suggesting that these wastes may serve as feedstocks for the creation of biopolymers like carboxymethyl cellulose (CMC).Item Effect of Raw and Delignified Banana Stem (Musa Cavendish) On the Rheological and Filtration Loss Properties of Water Based Mud(NJEAS, 2023-10-12) Ayuba Salihu; Ahmed Abubakar; Petrus Nzerem; Abdullahi Gimba; Khadijah Ibrahim; Ikechukwu Okafor; Khaleel JakadaIn compliance with environmental laws and safety rules, oil and gas companies have taken necessary steps to eradicate the use of toxic chemicals conventionally used in drilling muds, thereby promoting biodegradable alternatives. This research was carried out to investigate the effect of two banana stem samples; Raw Banana Stem (RBS) and Delignified Banana Stem (DBS) as potential and proficient viscosifiers and fluid loss control agents in water based mud. The rheological properties evaluated include plastic viscosity (cP), apparent viscosity (cP), yield point (Ib/100ft2) and gel strength (Ib/100ft2) at 10 seconds and 10 minutes. Filtration loss properties evaluated include filter cake thickness (mm) and fluid loss volume (ml). Each drilling mud sample was prepared using 350 ml, 20 g bentonite and varying contents (g) of carboxyl methyl cellulose (CMC), RBS and DBS. A mixer was used to mix the mud homogenously; the rheological properties were calculated using a viscometer while the filtration loss properties were calculated using a filter press. The results and analysis were compared to the effects of commercially available carboxymethyl cellulose to validate its properties. RBS and DBS improved the rheological properties of the mud sample contents of 3 g, 5 g, 7 g and 9 g. At contents of 5 g, 10 g, 15 g and 20 g, RBS and DBS samples provide significant fluid loss control and their results are similar to the results of CMC. RBS has a fluid loss volume increase of 6.84 %, 5.69 %, 17.12 % and 8.06 % from CMC’s results at slightly similar filter cake thickness while DBS has a fluid loss volume increase of 15.59 %, 15.09 %, 27.55 % and 15.35 % from CMC’s result. The data obtained from the experiments showed both banana samples can be used as environmentally friendly viscosifiers and fluid loss control agents.