Department of Petroleum & Gas

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Author: search.filters.author.Ikechukwu OkaforSubject: search.filters.subject.Drilling fluids

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    Evaluation of the Potential of Calcium Hydroxide Synthesized from Eggshells as a Drilling Fluid Additive
    (Petroleum and Coal, 2020-01-09) Abdullahi Gimba; Shalom Onome Amakhabi; Oghenerume Ogolo; Oluwaseun Alonge; Nzerem Petrus; Ikechukwu Okafor; David Afolayan
    This research work studied the suitability of Ca(OH)2 synthesized from eggshell as a drilling fluid additive. Ca(OH)2 was synthesized from calcined eggshells (CES) and uncalcined eggshells (UCES) and characterized using FTIR and EDX. Samples of one laboratory barrel of water-based mud were prepared using bentonite clay from Afuze, Edo State, Nigeria, and the synthesized Ca(OH)2 produced from CES and UCES and commercial Ca(OH)2 were added to different mud samples prepared, and its effect on the mud properties were tested for. The results obtained from the experiment conducted showed that the synthesized Ca(OH)2 gave comparable pH values as the commercial Ca(OH)2. Hence it served primarily as a pH enhancer. However, the addition of Ca(OH)2 from both sources increased the filtrate volume and mud cake thickness far beyond API standard which might create wellbore problems due to the high filtrate loss and mud cake thickness that were observed.
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    STUDY OF THE POTENTIAL OF CALCIUM HYDROXIDE SYNTHESIZED FROM PERIWINKLE SHELL AS A pH ENHANCER IN WATER BASED DRILLING MUD
    (NJEAS, 2023-01-01) Zainab Lamin; Ikechukwu Okafor; Khaleel Jakada; Petrus Nzerem; Abdullahi Gimba; Oghenerume Ogolo; Ayuba Salihu; Khadijah Ibrahim
    Reservoirs that contain acidic gases can lead to the corrosion of the drilling string and casing which could result in incessant down time and also increase the cost of drilling operation. This research work aimed at investigating the potential of using locally sourced materials such as Periwinkle Shell Ash (PSA) that can serve as substitutes to imported chemicals used in the industry, to help raise the mud pH to the API standard (9.5-12.5) whilst reducing the cost of drilling operation. Calcium hydroxide (Ca (OH2)) was extracted from Periwinkle Shell using two different process routes (via the calcination of the PSA and without it). Characterization tools were used to assess the functional groups present and the elemental composition of the periwinkle shell. Various laboratory equipment was used to observe the impact the additives would have on the mud properties (pH, mud weight, filtration characteristics and rheological properties) of the new drilling fluid. Results showed that as the mass of the synthesized Ca (OH2) from the calcined PSA, the uncalcined PSA and the commercial Ca (OH2) was increased, the pH of the mud samples was observed to have increased the pH of the base mud by 20.9%, 15.1% and 10%. Therefore, this research showed that the extracted Ca (OH2) acted primarily as a pH enhancer. However, the addition of Ca (OH2) from all sources exhibited poor filtration characteristics as there was high filtrate loss as the filtration time and the additive concentration increased which could affect the formulation and the performance of the drilling mud.