Research Articles in Petroleum & Gas

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    Performance Evaluation of Nanocellulose Synthesised from Yam Peels as a Fluid Loss Additive in Water Based Mud
    (Society of Petroleum Engineers, 2023-07-30) Khadijah Ibrahim; Petrus Nzerem; Ayuba Salihu; Abdullahi Gimba; Oghenerume Ogolo; Ajiri Otedheke; Rabiatu Adamu; Aisha Karofi
    Drilling fluids play a variety of roles in order to achieve a smooth and cost-effective drilling operation, the most important of which is their ability to seal permeable walls of the formation through the formation of a desirable mud cake, thereby reducing fluid loss. This study is targeted at evaluating the performance of nano cellulose, cellulose microfibrils synthesised from yam peels as a fluid loss additive and also its effect on the other properties of the drilling mud. The use of nano-cellulose is due to smaller particles forming better impermeable packing that will plug the permeable pore of the mud cake, as well as its ability to hold water. The nano cellulose was synthesised using bleaching, alkali treatment, and acid hydrolysis, and its quality was assessed using Fourier Transform Infrared Spectroscopy (FTIR) and Scanning Electron Microscopy, which confirmed the removal of some non-cellulose components as well as changes in surface morphology. The results of the experiment revealed that nano cellulose had an effect on the pH, rheological properties, and filtration properties of the drilling mud. The results also show that adding 1.5 g of nanocellulose reduced fluid loss by 8.13 %, and thus it can be concluded that yam peels nanocellulose will be an effective additive at higher concentrations compared to the Carboxyl Methyl Cellulose, a commercial additive.
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    STUDY OF THE POTENTIAL OF CALCIUM HYDROXIDE SYNTHESIZED FROM PERIWINKLE SHELL AS A pH ENHANCER IN WATER BASED DRILLING MUD
    (NJEAS, 2023-01-01) Zainab Lamin; Ikechukwu Okafor; Khaleel Jakada; Petrus Nzerem; Abdullahi Gimba; Oghenerume Ogolo; Ayuba Salihu; Khadijah Ibrahim
    Reservoirs that contain acidic gases can lead to the corrosion of the drilling string and casing which could result in incessant down time and also increase the cost of drilling operation. This research work aimed at investigating the potential of using locally sourced materials such as Periwinkle Shell Ash (PSA) that can serve as substitutes to imported chemicals used in the industry, to help raise the mud pH to the API standard (9.5-12.5) whilst reducing the cost of drilling operation. Calcium hydroxide (Ca (OH2)) was extracted from Periwinkle Shell using two different process routes (via the calcination of the PSA and without it). Characterization tools were used to assess the functional groups present and the elemental composition of the periwinkle shell. Various laboratory equipment was used to observe the impact the additives would have on the mud properties (pH, mud weight, filtration characteristics and rheological properties) of the new drilling fluid. Results showed that as the mass of the synthesized Ca (OH2) from the calcined PSA, the uncalcined PSA and the commercial Ca (OH2) was increased, the pH of the mud samples was observed to have increased the pH of the base mud by 20.9%, 15.1% and 10%. Therefore, this research showed that the extracted Ca (OH2) acted primarily as a pH enhancer. However, the addition of Ca (OH2) from all sources exhibited poor filtration characteristics as there was high filtrate loss as the filtration time and the additive concentration increased which could affect the formulation and the performance of the drilling mud.